Articles
  • Preparation of High-density YAG/ZrB2 Multi-phase Ceramics by Spark Plasma Sintering 
  • Jie-Guang Song, Jun-Guo Li, Jian-Rong Song and Lian-Meng Zhang*
  • State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China
Abstract
ZrB2 and YAG are widely applied because of some excellent properties, but ZrB2 is difficult to prepare as a high-density ceramic, and it is easily oxidized in high temperature air, which limits the application of ZrB2 materials. To obtain high-density for better oxidation resistance ZrB2 ceramic materials, in this paper, Al2O3 and Y2O3 are added into ZrB2 raw material to prepare high-density YAG/ZrB2 multi-phase ceramics by spark plasma sintering. Through the above analysis, it is proposed that 1600 degrees C is regarded as a critical sintering temperature (Tc) to fabricate YAG/ZrB2 multi-phase ceramics. Only if the sintering temperature is higher than Tic, can a nearly full density composite be achieved. The microstructure of sintered YAG/ZrB2 multi-phase ceramics after 4 minutes at 1600 degrees C is a better compact, the density and relative density are 5.5865 g/cm(3) and 99.40% respectively, which indicates that high-density YAG/ZrB2 multi-phase ceramics have been fabricated successfully.

Keywords: ZrB2; YAG multi-phase ceramics; densification behavior; relative density; spark plasma sintering

This Article

  • 2007; 8(5): 356-358

    Published on Oct 30, 2007