Articles
  • Effects of additives and sintering temperature on phase evolution and properties of carbon-clay ceramic composites
  • Fatai Olufemi Aramidea,b,*, O. D. Adepojua and Abimbola Patricia Popoolab
  • a Department of Metallurgical and Materials Engineering, Federal University of Technology, P.M.B. 704, Akure, Nigeria. b Department of Chemical, Metallurgical and Materials Engineering, Tshwane University of Technology, Staatsartillerie Road, Pretoria West, South Africa
Abstract
Effects of additives on phase development and physico-mechanical properties of mullite-carbon was investigated. Powdered clay, kaolinite and graphite of predetermined compositions were blended with additives using ball mill for 3 hrs at 60 rev/min. Samples were produced by uniaxial compression and sintered between 1400 oC and 1600 oC for one hr. They were characterized for various properties, developed phases and microstructural features. It was observed that the properties and phase developments in the samples were influenced by the additives. 10 wt % SiC served as nucleating point for SiC around 1400 oC. 10 wt % TiO2 lead to development of 2.5 wt % TiC at 1500 oC which increased to 6.8 wt % at 1600 oC. Ifon clay in the sample leads to development of anorthite and microcline in the samples. 10 wt % TiO2 is effective as anti-oxidant for graphite up to 1500 oC. Base on strength and absorbed energy, sample C (with 10 wt % TiO2) sintered at 1500 oC is considered to be optimum.

Keywords: Additives, Ceramic composite, Carbon-clay, Phase development, Mullite

This Article

  • 2018; 19(6): 483-491

    Published on Dec 31, 2018