Articles
  • Heating and phyiso-mechanical characteristics of porous spinel developed by Starch 
  • Kumar Saurav*, Manas Ranjan Majhi and Vinay Kumar Singh
  • Department of Ceramic Engineering, Indian Institute of Technology (BHU), India
Abstract
Among the techniques used to produce these materials (such as the addition of foaming agents and organic compounds), thepore generation via phase transformation presents key aspects, such as easy processing and the absence of toxic volatiles. Inthis study, this technique was applied to produce porous ceramics by decomposing an EX potato known as starch soluble(C6H10O5)n. Porous MgO ceramics prepared at different sintering temperatures is studied. Porous MgO was synthesis byheating pellets at 1100 oC for 1hr. The resultant porous MgO was then immersed in an 10 mol/L aluminium nitrate solution,dried, and reheated at 1300 oC for 2 hrs to convert it to spinel. The method results from generalized relations that weredesigned for study of physical properties of fractal structures. As it is shown these relations are in a good agreement with theequations used for the description of time responses of temperature for the pulse input of supplied heat. The volume fractionof porosity can be defined as the fraction of void space relative to the apparent total bulk volume of the sample. Porosity inmaterials originates from different processing and synthesis routes.

Keywords: Ceramics, Thermo Gravimetric analysis (TGA), Chemical synthesis, Mechanical properties, Microstructure

This Article

  • 2016; 17(10): 1019-1023

    Published on Oct 31, 2016