Articles
  • Characterization of SiC powders synthesized from rice husks and fused silica powder by carbothermal reduction reaction
  • Young-Hoon Yun*

  • Dept. of New & Renewable Energy, Dongshin University, Naju, 58245, Korea

  • This article is an open access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/4.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

Fine β-SiC powders were synthesized from rice husks and fused silica powder. In this SiC powder synthesis, carbon flakes were carbonized by heating rice husks with silica powder, and then the carbon flakes underwent a secondary reaction with the SiO vapor formed by the carbothermal reduction reaction. The SiC powders obtained from carbonized rice husks and fused silica powder were characterized by XRD, XPS, SEM and TEM. In the XRD patterns, the spectra clearly showed very strong peaks for the (111) plane near 35o and weak (220) and (311) peaks at approximately 60o and 72o, respectively. According to the XRD pattern, the powder synthesized from a 6:4 mixture of carbonized rice husks and silica under an Ar atmosphere contained mainly cubic crystalline SiC and a relatively small amount of a hexagonal phase without residual carbon. TEM images and FFT pattern showed that this specimen contained relatively fine particles (under 0.5 µm) and a crystalline 3C-SiC phase with a (100) diffraction pattern


Keywords: Silicon carbide (SiC), Rice husks, Silica, Carbothermal reduction

This Article

  • 2022; 23(3): 247-251

    Published on Jun 30, 2022

  • 10.36410/jcpr.2022.23.3.247
  • Received on Jul 20, 2021
  • Revised on Feb 3, 2022
  • Accepted on Mar 3, 2022

Correspondence to

  • Young-Hoon Yun
  • Dept. of New & Renewable Energy, Dongshin University, Naju, 58245, Korea
    Tel : +82-61-330-7633 Fax: +82-61-330-2909

  • E-mail: yunh2@dsu.ac.kr