Articles
  • Preparation and characterization of Alumina / Magnesia / Zirconia / Graphite refractory composites using response surface methodology
  • Maryam Abolfazli and Mohammad Hossein Paydar*

  • Department of Materials Science and Engineering, School of Engineering, Shiraz University, Shiraz, Iran

  • This article is an open access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/4.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

In the present study, Alumina/ Magnesia/ Zirconia/ Graphite (AMZG) refractory composite was fabricated and its physical, mechanical and chemical properties were investigated. The preparation of AMZG refractory composite was modeled and optimized by using Central Composite Design (CCD). Among all factors, zirconia content (0-5 wt.%), magnesia content (0-10 wt.%) and graphite size (fine and coarse grained) were selected. The factors were varied in 5 levels and the responses were fitted by quadratic regression model. Statistical data showed that the highest relative density, modulus of rupture and oxidation resistance were obtained by fine grained graphite at zirconia and magnesia of 3.312 wt.% and 4.075 wt.%, respectively. Quantitative analysis of the X-ray diffraction (XRD) pattern by Rietveld method revealed that the optimal sample composition included 44.2, 26.1, 10.3, 4.2 and 15.2 wt% of corundum, cordierite, spinel, zirconium oxide and graphite phases, respectively. The result of XRD is confirmed by Differential Thermal Analysis (DTA). The oxidation resistance (at 900 oC) of the best specimen was investigated


Keywords: Alumina/Magnesia/Zirconia/graphite composites, Refractories, Microstructure, Mechanical properties, Oxidation resistance, Response surface methodology

This Article

  • 2022; 23(2): 188-198

    Published on Apr 30, 2022

  • 10.36410/jcpr.2022.23.2.188
  • Received on Oct 3, 2021
  • Revised on Nov 10, 2021
  • Accepted on Nov 27, 2021

Correspondence to

  • Mohammad Hossein Paydar
  • Department of Materials Science and Engineering, School of Engineering, Shiraz University, Shiraz, Iran
    Tel : +98-71-32307293 Fax: +98-7132307293

  • E-mail: paaydar@shirazu.ac.ir